Proceedings of the Fifth Conference on Carbon by Yong Zhou

By Yong Zhou

Complaints of the 5th convention on Carbon

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This is why our efforts were directed to find a technique which would permit us to control the formation of spin centers in carbons. 9 There was, how­ ever, some evidence that spin centers are created in chars by chemical attack. 5 Furthermore, Mrozowski and Wobschall6 ob­ served an increase in spin concentration when 10 G. Wagoner, Proc. Fourth Carbon Conf. Pergamon Press (1960) p . 197. 11 G. R. Hennig and B . Smaller, Proc. First and Second Carbon Conf. University of Buffalo (1956) p. 113. a C3S2 polymer was heat treated in air and Blayden and Patrick 12 observed' also an increase in spin concentration resulting from a short exposure of a char to sulfur vapor at a temperature around 500°C.

II faut remarquer, qu'afin de ne pas perturber les lignes d'induction magnetique, ni le cadre, ni le pot de presse ne comportent de pieces ferromagnetiques. 3. L'electro-aimant (Fig. 5). On utilise un electro-aimant "Varian" — modele V 4007 avec une alimentation stabilisee modele V 2200, specialement concue pour ce type d'appareil. Dans l'entrefer de 32 mm employe, cet electro-aimant donne une induction de 1,0120 Weber m~ 2 . L'uniformite du champ est assure ä mieux de 1 % pres dans un cercle de diametre 120 m m concentrique des pieces polaires.

The broadening is ascribed to the perturbing influence of the magnetic moments of the oxygen molecules. 14 Oxygen sensitivity of spin centers as strong as for chars was found in this work when centers were formed by oxidation in car­ bonized materials heat treated to temperature equal or below 1000°C. The oxygen sensitivity was checked by introducing air into the sample. For such carbons the atmospheric oxygen broadens the line so much t h a t the line 14 D. J. E.

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